Certificate of Analysis

Produced: Aug 02, 2023

Entourage Day Gummies 100mg - Sour Citrus (Edible Solid) // Client: Forever 46 LLC

Batch Result: Pass

Batch No.: 230104-001-ESC

Cultivar: Hybrid Blend

Matrix: Edible Solid

Category: Edible

Sample ID: TLT-230727-003

Collected on: Jul 27, 2023

Received on: Jul 27, 2023

Batch Size: 1500 Units

Sample Size: 56 g

Received By: Raul Manuel Morales Jr

59.92 mg/pkg

54.32 mg/pkg

218.4 mg/pkg

Microbial

Pass

Mycotoxins

Pass

Pesticides

Pass

Cannabinoids

Heavy Metals

Pass

Residual Solvents

Pass

Cultivator

Forever 46 LLC

License

00000057DCHF00477864

Type

Medicinal - Cultivator License

https://lims.tagleaf.com/coas/oW7kJu2az5wU7M3eblxIEUNmFS3k8LUeKiUwlDY0PBizalPmgK

Results Certified By: William English

Lab Director, Titan Laboratories

Aug 02, 2023

SOP 50: Cannabinoid Profile by HPLC-MS Aug 02, 2023

Analyte	Detected	Detected	LOD	LOQ
CBD	0.096 %	0.96 mg/g	0.010 mg/g	0.031 mg/g
CBDA	ND	ND	0.010 mg/g	0.031 mg/g
CBG	0.097 %	0.97 mg/g	0.010 mg/g	0.031 mg/g
CBN	0.004 %	0.04 mg/g	0.010 mg/g	0.031 mg/g
Δ⁸-THC	0.107 %	1.07 mg/g
Δ⁹-THC	0.086 %	0.86 mg/g	0.010 mg/g	0.031 mg/g
THCA	ND	ND	0.010 mg/g	0.031 mg/g
Total THC (Total THC = (THCA x 0.877) + Delta-9-THC)	0.086 %	0.86 mg/g
Total CBD (Total CBD = (CBDA x 0.877) + CBD)	0.096 %	0.96 mg/g
CBD Per Package Package: 56 Grams	53.760 Milligrams
Δ⁹-THC Per Package Package: 56 Grams	48.160 Milligrams
Total THC Per Package Package: 56 Grams	48.160 Milligrams
Total CBD Per Package Package: 56 Grams	53.760 Milligrams

SOP 50: Expanded Cannabinoid Profile by HPLC-MS Aug 02, 2023

Analyte	Detected	Detected
CBC	ND	ND
CBCA	ND	ND
CBGA	ND	ND

SOP 130: E. coli by 3M Petrifilm Jul 28, 2023

Analyte	Limit	Detected	Pass/Fail
Escherichia coli	100 CFU/g	ND	Pass

SOP 120: Salmonella by Gene-Up qPCR Jul 28, 2023

Analyte	Limit	Detected	Pass/Fail
Salmonella spp.	Any amount in 1 gram	ND	Pass

SOP 60: Mycotoxins by LC-MS/MS Jul 31, 2023

Analyte	Limit	Detected	Pass/Fail
Aflatoxin B1		ND
Aflatoxin B2		ND
Aflatoxin G1		ND
Aflatoxin G2		ND
Aflatoxins	20 µg/kg	ND	Pass
Ochratoxin A	20 µg/kg	ND	Pass

SOP 60: Pesticides by LC-MS/MS Aug 02, 2023

Analyte	Limit	Detected	Pass/Fail
Abamectin	0.5 µg/g	ND	Pass
Acephate	0.4 µg/g	ND	Pass
Acequinocyl	2 µg/g	ND	Pass
Acetamiprid	0.2 µg/g	ND	Pass
Aldicarb	0.4 µg/g	ND	Pass
Azoxystrobin	0.2 µg/g	ND	Pass
Bifenazate	0.2 µg/g	ND	Pass
Bifenthrin	0.2 µg/g	ND	Pass
Boscalid	0.4 µg/g	ND	Pass
Carbaryl	0.2 µg/g	ND	Pass
Carbofuran	0.2 µg/g	ND	Pass
Chlorantranil- iprole	0.2 µg/g	ND	Pass
Chlorfenapyr	1 µg/g	ND	Pass
Chlorpyrifos	0.2 µg/g	ND	Pass
Clofentezine	0.2 µg/g	ND	Pass
Cyfluthrin	1 µg/g	ND	Pass
Cypermethrin	1 µg/g	ND	Pass
Daminozide	1 µg/g	ND	Pass
Diazinon	0.2 µg/g	ND	Pass
Dichlorvos	0.1 µg/g	ND	Pass
Dimethoate	0.2 µg/g	ND	Pass
Ethoprophos	0.2 µg/g	ND	Pass
Etofenprox	0.4 µg/g	ND	Pass
Etoxazole	0.2 µg/g	ND	Pass
Fenoxycarb	0.2 µg/g	ND	Pass
Fenpyroximate	0.4 µg/g	ND	Pass
Fipronil	0.4 µg/g	ND	Pass
Flonicamid	1 µg/g	ND	Pass
Fludioxonil	0.4 µg/g	ND	Pass

Analyte	Limit	Detected	Pass/Fail
Hexythiazox	1 µg/g	ND	Pass
Imazalil	0.2 µg/g	ND	Pass
Imidacloprid	0.4 µg/g	ND	Pass
Kresoxim- methyl	0.4 µg/g	ND	Pass
Malathion	0.2 µg/g	ND	Pass
Metalaxyl	0.2 µg/g	ND	Pass
Methiocarb	0.2 µg/g	ND	Pass
Methomyl	0.4 µg/g	ND	Pass
Myclobutanil	0.2 µg/g	ND	Pass
Naled	0.5 µg/g	ND	Pass
Oxamyl	1 µg/g	ND	Pass
Paclobutrazol	0.4 µg/g	ND	Pass
Permethrin	0.2 µg/g	ND	Pass
Phosmet	0.2 µg/g	ND	Pass
Piperonylbuto- xide	2 µg/g	ND	Pass
Prallethrin	0.2 µg/g	ND	Pass
Propiconazole	0.4 µg/g	ND	Pass
Propoxur	0.2 µg/g	ND	Pass
Pyrethrins	1 µg/g	ND	Pass
Pyridaben	0.2 µg/g	ND	Pass
Spinosad	0.2 µg/g	ND	Pass
Spiromesifen	0.2 µg/g	ND	Pass
Spirotetramat	0.2 µg/g	ND	Pass
Spiroxamine	0.4 µg/g	ND	Pass
Tebuconazole	0.4 µg/g	ND	Pass
Thiacloprid	0.2 µg/g	ND	Pass
Thiamethoxam	0.2 µg/g	ND	Pass
Trifloxystrob- in	0.2 µg/g	ND	Pass

SOP 70: Heavy Metals by ICP-MS Jul 28, 2023

Analyte	Limit	Detected	Pass/Fail
Arsenic	0.4 µg/g	0.005 µg/g	Pass
Cadmium	0.4 µg/g	0.005 µg/g	Pass
Lead	1 µg/g	0.139 µg/g	Pass
Mercury	1.2 µg/g	0.026 µg/g	Pass

SOP 80: Residual Solvents by GC-MS Aug 01, 2023

Analyte	Limit	Detected	Pass/Fail
2,2- Dimethylbutane		ND
2,3- Dimethylbutane		ND
2- Methylpentane		ND
3- Methylpentane		ND
Acetone	1000 µg/g	ND	Pass
Acetonitrile	410 µg/g	ND	Pass
Benzene	2 µg/g	ND	Pass
Butane		ND
Butanes	5000 µg/g	ND	Pass
Chloroform	60 µg/g	ND	Pass
Dichlorometha- ne	600 µg/g	ND	Pass
Ethanol	5000 µg/g	ND	Pass
Ethyl acetate	5000 µg/g	ND	Pass
Ethylbenzene		ND
Ethyl ether	5000 µg/g	ND	Pass
Heptane	5000 µg/g	ND	Pass
Hexane		ND
Hexanes	290 µg/g	ND	Pass
Isobutane		ND
Isopentane		ND
Isopropyl acetate	5000 µg/g	ND	Pass
Isopropyl alcohol	5000 µg/g	ND	Pass
Methanol	3000 µg/g	ND	Pass
Neopentane		ND
Pentane		ND
Pentanes	5000 µg/g	ND	Pass
Propane	5000 µg/g	ND	Pass
Toluene	890 µg/g	ND	Pass
o-Xylene		ND
p- and m-Xylene		ND
Total xylenes	2170 µg/g	ND	Pass