Certificate of Analysis

Completed: Jan 08, 2024

Pineapple Express, 2.5g Pre-Rolls (Infused Pre-Roll) // Client: Ironworks Collective, Inc.

Batch Result: Pass

Batch No.: ST-40MPEX-P0623

Matrix: Pre-roll

Category: Inhalable

Sample ID: CTL-240105-021

Batch Date: Dec 06, 2023

Collected on: Jan 05, 2024

Received on: Jan 05, 2024

Batch Size: 11988 Units

Sample Size: 32 Units

41.779 %

0.000 %

42.719 %

44.226 %

Moisture

Microbial

Pass

Mycotoxins

Pass

Pesticides

Pass

Cannabinoids

Heavy Metals

Pass

Water Activity

Pass

Foreign Materials

Pass

Residual Solvents

Pass

Manufacturer

Ironworks Collective, Inc.

License

CDPH-10003246

Type

Adult-Use and Medicinal - Manufacturing License

Distributor

Ironworks Collective, Inc.

License

C11-0000620-LIC

Type

Adult-Use and Medicinal - Distributor License

https://lims.tagleaf.com/coas/8wB0R0024j0Qo0fXWc8TwZEKVPmDBZuSwDopdxhiBgRf7kpgXT

This product has been tested by California Cannabis Testing Lab (CCTL) using valid testing methodologies and a quality system as required by state law. Values reported relate only to the product tested. CCTL makes no claims as to the efficacy, safety, or other risks associated with any detected or non-detected levels of any compounds reported herein. This certificate shall not be reproduced except in full without the written approval of CCTL. Samples were collected as per 4 CCR Section 15707.

Results Certified By: James W. Cox

Laboratory Director

Jan 08, 2024

Cannabinoids by HPLC: CCTL-PM-002, SOP-011 Jan 06, 2024

Dry-weight amounts shown

Analyte	Detected	Detected	LOD	LOQ	Pass/Fail
CBC	0.212 %	2.12 mg/g	0.2444 mg/g	0.4888 mg/g	N/A
CBD	ND	ND	0.2444 mg/g	0.4888 mg/g	N/A
CBDA	ND	ND	0.2444 mg/g	0.4888 mg/g	N/A
CBDV	ND	ND	0.2444 mg/g	0.4888 mg/g	N/A
CBG	0.669 %	6.69 mg/g	0.2444 mg/g	0.4888 mg/g	N/A
CBGA	0.067 %	0.67 mg/g	0.2444 mg/g	0.4888 mg/g	N/A
CBN	ND	ND	0.2444 mg/g	0.4888 mg/g	N/A
Δ⁸-THC	ND	ND	0.2444 mg/g	0.4888 mg/g	N/A
Δ⁹-THC	31.091 %	310.91 mg/g	0.2444 mg/g	0.4888 mg/g	N/A
THCA	12.187 %	121.87 mg/g	0.2444 mg/g	0.4888 mg/g	N/A
THCV	ND	ND	0.2444 mg/g	0.4888 mg/g	N/A
Total THC (Total THC = Delta-8-THC + (Delta-8-THCA x 0.877) + Delta-9-THC + (THCA x 0.877))	41.779 %	417.79 mg/g			N/A
Total CBD (Total CBD = CBD + (CBDA x 0.877))	ND	ND			N/A
CBD Per Package Package: 2.5 Grams	ND				N/A
Δ⁹-THC Per Package Package: 2.5 Grams	777.275 Milligrams				N/A
Total THC Per Package Package: 2.5 Grams	1044.475 Milligrams				N/A
Total CBD Per Package Package: 2.5 Grams	ND				N/A

Moisture Content: SOP-009 Jan 05, 2024

Analyte	Limit	Detected	Pass/Fail
Moisture		10.650 %	N/A

Microbials: SOP-016, SOP-017 Jan 06, 2024

Analyte	Limit	Detected	Pass/Fail
Aspergillus flavus	Any amount in 1 gram	ND	Pass
Aspergillus fumigatus	Any amount in 1 gram	ND	Pass
Aspergillus niger	Any amount in 1 gram	ND	Pass
Aspergillus terreus	Any amount in 1 gram	ND	Pass
Salmonella spp.	Any amount in 1 gram	ND	Pass
Shiga toxin-producing E. coli	Any amount in 1 gram	ND	Pass

Mycotoxins by LCMS: CCTL-PM-020 Jan 06, 2024

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Aflatoxin B1		ND	1.465 µg/kg	2.929 µg/kg	N/A
Aflatoxin B2		ND	2.937 µg/kg	5.874 µg/kg	N/A
Aflatoxin G1		ND	1.465 µg/kg	2.929 µg/kg	N/A
Aflatoxin G2		ND	1.465 µg/kg	2.929 µg/kg	N/A
Aflatoxins	20 µg/kg	ND			Pass
Ochratoxin A	20 µg/kg	ND	5.859 µg/kg	11.718 µg/kg	Pass

Pesticides by LCMS: CCTL-PM-030 Jan 06, 2024

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Abamectin	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Acephate	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Acequinocyl	0.1 µg/g	ND	0.0119 µg/g	0.0238 µg/g	Pass
Acetamiprid	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Aldicarb	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Azoxystrobin	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Bifenazate	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Bifenthrin	3 µg/g	ND	0.0238 µg/g	0.0476 µg/g	Pass
Boscalid	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Carbaryl	0.5 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Carbofuran	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Chlorantranil- iprole	10 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Chlorpyrifos	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Clofentezine	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Coumaphos	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Cyfluthrin	2 µg/g	ND	0.0235 µg/g	0.0470 µg/g	Pass
Cypermethrin	1 µg/g	ND	0.0117 µg/g	0.0235 µg/g	Pass
Daminozide	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Diazinon	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Dichlorvos	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Dimethoate	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Dimethomorph	2 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Ethoprophos	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Etofenprox	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Etoxazole	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Fenhexamid	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Fenoxycarb	Any amount	ND	0.0119 µg/g	0.0238 µg/g	Pass
Fenpyroximate	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Fipronil	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Flonicamid	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Fludioxonil	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Hexythiazox	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Imazalil	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Imidacloprid	5 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Kresoxim- methyl	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Malathion	0.5 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Metalaxyl	2 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Methiocarb	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Methomyl	1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Mevinphos	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Myclobutanil	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Naled	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Oxamyl	0.5 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Paclobutrazol	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Permethrin	0.5 µg/g	ND	0.0238 µg/g	0.0476 µg/g	Pass
Phosmet	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Piperonylbuto- xide	3 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Prallethrin	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Propiconazole	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Propoxur	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Pyrethrins	0.5 µg/g	ND			Pass
Pyrethrins Pyrethrin I		ND	0.0059 µg/g	0.0117 µg/g	N/A
Pyrethrins Pyrethrin II		ND	0.0059 µg/g	0.0117 µg/g	N/A
Pyridaben	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Spinetoram	0.1 µg/g	ND			Pass
Spinetoram J		ND	0.0059 µg/g	0.0117 µg/g	N/A
Spinetoram L		ND	0.0059 µg/g	0.0117 µg/g	N/A
Spinosad	0.1 µg/g	ND			Pass
Spinosad A		ND	0.0059 µg/g	0.0117 µg/g	N/A
Spinosad D		ND	0.0059 µg/g	0.0117 µg/g	N/A
Spiromesifen	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Spirotetramat	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Spiroxamine	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Tebuconazole	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Thiacloprid	Any amount	ND	0.0059 µg/g	0.0117 µg/g	Pass
Thiamethoxam	5 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass
Trifloxystrob- in	0.1 µg/g	ND	0.0059 µg/g	0.0117 µg/g	Pass

Pesticides by GCMS: CCTL-PM-020 Jan 06, 2024

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Captan	0.7 µg/g	ND	0.2392 µg/g	0.4784 µg/g	Pass
Chlordane	Any amount	ND			Pass
Chlordane cis		ND	0.0149 µg/g	0.0299 µg/g	N/A
Chlordane trans		ND	0.0149 µg/g	0.0299 µg/g	N/A

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Chlorfenapyr	Any amount	ND	0.0299 µg/g	0.0597 µg/g	Pass
Methyl parathion	Any amount	ND	0.0304 µg/g	0.0609 µg/g	Pass
Pentachloroni- trobenzene	0.1 µg/g	ND	0.0304 µg/g	0.0609 µg/g	Pass

Heavy Metals by ICP-MS: CCTL-PM-005 Jan 05, 2024

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Arsenic	0.2 µg/g	ND	0.050 µg/g	0.100 µg/g	Pass
Cadmium	0.2 µg/g	ND	0.050 µg/g	0.100 µg/g	Pass
Lead	0.5 µg/g	ND	0.050 µg/g	0.100 µg/g	Pass
Mercury	0.1 µg/g	ND	0.010 µg/g	0.020 µg/g	Pass

Water Activity: CCTL-PM-028, SOP-009 Jan 05, 2024

Analyte	Limit	Detected	Pass/Fail
Water Activity	0.65 Aw	0.471 Aw	Pass

Foreign Matter: CCTL-PM-003 Jan 05, 2024

Analyte	Limit	Detected	Pass/Fail
Imbedded Foreign Material	25 %	ND	Pass
Insect Fragments, Hair, Mammal Excrement	1 Unit	ND	Pass
Mold	25 %	ND	Pass
Sand, Soil, Cinders, Dirt	25 %	ND	Pass

Residual Solvents by GCMS: CCTL-PM-010 Jan 06, 2024

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
1,2- Dichloroethane	1 µg/g	ND	0.147 µg/g	0.294 µg/g	Pass
Acetone	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Acetonitrile	410 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Benzene	1 µg/g	ND	0.147 µg/g	0.294 µg/g	Pass
Butane	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Chloroform	1 µg/g	ND	0.147 µg/g	0.294 µg/g	Pass
Ethanol	5000 µg/g	< LOQ	23.438 µg/g	46.875 µg/g	Pass
Ethyl acetate	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Ethylene oxide	1 µg/g	ND	0.147 µg/g	0.294 µg/g	Pass
Ethyl ether	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Heptane	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Hexane	290 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Isopropyl alcohol	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Methanol	3000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Methylene chloride	1 µg/g	ND	0.147 µg/g	0.294 µg/g	Pass
Pentane	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Propane	5000 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Toluene	890 µg/g	ND	23.438 µg/g	46.875 µg/g	Pass
Trichloroethy- lene	1 µg/g	ND	0.147 µg/g	0.294 µg/g	Pass
o-Xylene		ND	11.719 µg/g	23.438 µg/g	N/A
p- and m-Xylene		ND	11.719 µg/g	23.438 µg/g	N/A
Total xylenes	2170 µg/g	ND			Pass

Certificate of Analysis

Cannabinoids by HPLC: CCTL-PM-002, SOP-011 Jan 06, 2024

Moisture Content: SOP-009 Jan 05, 2024

Microbials: SOP-016, SOP-017 Jan 06, 2024

Mycotoxins by LCMS: CCTL-PM-020 Jan 06, 2024

Pesticides by LCMS: CCTL-PM-030 Jan 06, 2024

Pesticides by GCMS: CCTL-PM-020 Jan 06, 2024

Heavy Metals by ICP-MS: CCTL-PM-005 Jan 05, 2024

Water Activity: CCTL-PM-028, SOP-009 Jan 05, 2024

Foreign Matter: CCTL-PM-003 Jan 05, 2024

Residual Solvents by GCMS: CCTL-PM-010 Jan 06, 2024

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