Certificate of Analysis

* For quality assurance purposes. Not a California compliance certificate.

Produced: Jul 07, 2023

FRYD-MIXED SAMPLES (Concentrate) // Client: A.Nonymous

Batch Result: Fail

DISPOSABLE VAPE PEN

Batch No.: WILD BAJA BLAST

Matrix: Concentrate

Category: Inhalable

Sample ID: BCL-230703-003

Collected on: Jul 03, 2023

Received on: Jul 03, 2023

Batch Size:

Sample Size: 10 Units

78.55359 %

0.4011 %

85.39591 %

85.9448 %

Mycotoxins

Pass

Pesticides

Fail

Terpenoids

Cannabinoids

Heavy Metals

Pass

Foreign Materials

Pass

Residual Solvents

Pass

https://lims.tagleaf.com/coas/2nMm1ZuX51ffxesL0Ch69xc6gZ8XhHqnspVJpa5Qg2iuXgPkAI

Sample was tested as received. The results relate only to the items tested. All LQC samples required by section 15730 of California Code of Regulations Title 4 Division 19 Department of Cannabis Control were performed and met the acceptance criteria. All decision rules are established by the DCC.

Results Certified By: Dzoana Klisara, B.Sc.

Laboratory Director, BelCosta Labs

Jul 07, 2023

BCL-03: Cannabinoid Potency by HPLC-UV Jul 06, 2023

† Sum of Cannabinoids = CBC + CBCA + CBD + CBDA + CBDV + CBDVA + CBG + CBGA + CBN + Delta-8-THC + Delta-9-THC + THCA + THCV + THCVA

†† Total Cannabinoids = (CBC + CBD + CBDV + CBG + CBN + Delta-8-THC + Delta-9-THC + THCV) + (0.877 * (CBCA + CBDA + CBDVA + CBGA + THCA + THCVA))

Analyte	Detected	Detected	LOD	LOQ	Pass/Fail
CBC	1.294 %	12.94 mg/g	0.022 mg/g	0.5 mg/g	N/A
CBCA	0.1428 %	1.428 mg/g	0.063 mg/g	0.5 mg/g	N/A
CBD	0.4011 %	4.011 mg/g	0.031 mg/g	0.5 mg/g	N/A
CBDA	ND	ND	0.016 mg/g	0.5 mg/g	N/A
CBDV	ND	ND	0.024 mg/g	0.5 mg/g	N/A
CBDVA	ND	ND	0.016 mg/g	0.5 mg/g	N/A
CBG	2.3536 %	23.536 mg/g	0.029 mg/g	0.5 mg/g	N/A
CBGA	0.2619 %	2.619 mg/g	0.02 mg/g	0.5 mg/g	N/A
CBN	1.9171 %	19.171 mg/g	0.016 mg/g	0.5 mg/g	N/A
Δ⁸-THC	ND	ND	0.058 mg/g	0.5 mg/g	N/A
Δ⁹-THC	74.9949 %	749.949 mg/g	0.042 mg/g	0.5 mg/g	N/A
THCA	4.0578 %	40.578 mg/g	0.03 mg/g	0.5 mg/g	N/A
THCV	0.5216 %	5.216 mg/g	0.033 mg/g	0.5 mg/g	N/A
THCVA	ND	ND	0.023 mg/g	0.5 mg/g	N/A
Total THC (Total THC = Delta-8-THC + (Delta-8-THCA x 0.877) + Delta-9-THC + (THCA x 0.877))	78.55359 %	785.5359 mg/g			N/A
Total CBD (Total CBD = CBD + (CBDA x 0.877))	0.4011 %	4.011 mg/g			N/A

BCL-09: Terpenoid Testing by HS-GC/FID Jul 06, 2023

Analyte	Detected	Detected	LOD	LOQ	Pass/Fail
Total Terpenes	3.82325 %	38.2325 mg/g			N/A
d-Limonene	1.45432 %	14.5432 mg/g	0.00025 mg/g	0.13731 mg/g	N/A
β-Caryophyllene	0.68569 %	6.8569 mg/g	0.00188 mg/g	0.13731 mg/g	N/A
β-Myrcene	0.56361 %	5.6361 mg/g	0.00037 mg/g	0.13731 mg/g	N/A
Linalool	0.34344 %	3.4344 mg/g	0.00036 mg/g	0.13731 mg/g	N/A
α-Humulene	0.21573 %	2.1573 mg/g	0.00046 mg/g	0.13731 mg/g	N/A
α-Pinene	0.17404 %	1.7404 mg/g	0.00021 mg/g	0.13731 mg/g	N/A
β-Pinene	0.13181 %	1.3181 mg/g	0.00222 mg/g	0.13731 mg/g	N/A
α-Bisabolol	0.10096 %	1.0096 mg/g	0.00428 mg/g	0.13731 mg/g	N/A
Terpinolene	0.03529 %	0.3529 mg/g	0.00029 mg/g	0.13731 mg/g	N/A
γ-Terpinene	0.03161 %	0.3161 mg/g	0.00046 mg/g	0.13731 mg/g	N/A
cis-β-Ocimene	0.02805 %	0.2805 mg/g	0.00133 mg/g	0.04257 mg/g	N/A
Camphene	0.0249 %	0.249 mg/g	0.00021 mg/g	0.13731 mg/g	N/A
Geraniol	0.02363 %	0.2363 mg/g	0.00029 mg/g	0.13731 mg/g	N/A
trans-β-Ocimene	0.01017 %	0.1017 mg/g	0.00049 mg/g	0.09474 mg/g	N/A
α-Terpinene	< LOQ	< LOQ	0.0003 mg/g	0.13731 mg/g	N/A
Guaiol	< LOQ	< LOQ	0.00268 mg/g	0.13731 mg/g	N/A
Δ³-Carene	ND	ND	0.00045 mg/g	0.13731 mg/g	N/A
Eucalyptol	ND	ND	0.00046 mg/g	0.13731 mg/g	N/A
Isopulegol	ND	ND	0.00054 mg/g	0.13731 mg/g	N/A
p-Cymene	ND	ND	0.00027 mg/g	0.13731 mg/g	N/A

BCL-11: Mycotoxin Testing by LC-MS/MS Jul 07, 2023

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Aflatoxin B1		ND	1.97 µg/kg	5.96 µg/kg	N/A
Aflatoxin B2		ND	1.32 µg/kg	3.99 µg/kg	N/A
Aflatoxin G1		ND	1.6 µg/kg	4.86 µg/kg	N/A
Aflatoxin G2		ND	1.46 µg/kg	4.44 µg/kg	N/A
Aflatoxins	20 µg/kg	ND			Pass
Ochratoxin A	20 µg/kg	ND	1.35 µg/kg	4.08 µg/kg	Pass

BCL-13: Pesticide Testing by GC/MS Jul 07, 2023

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Captan	0.7 µg/g	ND	0.03075 µg/g	0.09314 µg/g	Pass
Chlordane	Any amount	0.1915 µg/g			Fail
Chlordane cis		0.0893 µg/g	0.01088 µg/g	0.03298 µg/g	N/A
Chlordane trans		0.1022 µg/g	0.01041 µg/g	0.03146 µg/g	N/A
Chlorfenapyr	Any amount	6.9333 µg/g	0.02345 µg/g	0.07098 µg/g	Fail

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Chlorpyrifos	Any amount	0.5091 µg/g	0.01093 µg/g	0.03321 µg/g	Fail
Dichlorvos	Any amount	ND	0.01152 µg/g	0.03491 µg/g	Pass
Methyl parathion	Any amount	ND	0.01321 µg/g	0.04005 µg/g	Pass
Pentachloroni- trobenzene	0.1 µg/g	ND	0.01374 µg/g	0.04169 µg/g	Pass

BCL-05: Residual Pesticide Analysis by LC-MS/MS ESI Jul 07, 2023

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Abamectin	0.1 µg/g	ND	0.0244 µg/g	0.07393 µg/g	Pass
Acephate	0.1 µg/g	ND	0.01224 µg/g	0.0371 µg/g	Pass
Acequinocyl	0.1 µg/g	ND	0.01993 µg/g	0.06038 µg/g	Pass
Acetamiprid	0.1 µg/g	ND	0.0043 µg/g	0.01302 µg/g	Pass
Aldicarb	Any amount	ND	0.01219 µg/g	0.03693 µg/g	Pass
Azoxystrobin	0.1 µg/g	ND	0.00771 µg/g	0.02337 µg/g	Pass
Bifenazate	0.1 µg/g	21.3862 µg/g	0.00373 µg/g	0.01131 µg/g	Fail
Bifenthrin	3 µg/g	1.481 µg/g	0.01267 µg/g	0.03839 µg/g	Pass
Boscalid	0.1 µg/g	ND	0.01406 µg/g	0.04261 µg/g	Pass
Carbaryl	0.5 µg/g	ND	0.00615 µg/g	0.01865 µg/g	Pass
Carbofuran	Any amount	ND	0.00411 µg/g	0.01246 µg/g	Pass
Chlorantranil- iprole	10 µg/g	ND	0.01069 µg/g	0.0324 µg/g	Pass
Clofentezine	0.1 µg/g	ND	0.01404 µg/g	0.04256 µg/g	Pass
Coumaphos	Any amount	ND	0.01952 µg/g	0.05914 µg/g	Pass
Cyfluthrin	2 µg/g	ND	0.1511 µg/g	0.45788 µg/g	Pass
Cypermethrin	1 µg/g	1.9003 µg/g	0.02284 µg/g	0.06921 µg/g	Fail
Daminozide	Any amount	< LOQ	0.0237 µg/g	0.07182 µg/g	Fail
Diazinon	0.1 µg/g	0.0154 µg/g	0.0027 µg/g	0.00818 µg/g	Pass
Dimethoate	Any amount	0.0401 µg/g	0.00353 µg/g	0.01069 µg/g	Fail
Dimethomorph	2 µg/g	ND			Pass
Dimethomorph I		ND	0.00554 µg/g	0.01679 µg/g	N/A
Dimethomorph II		ND	0.00327 µg/g	0.00992 µg/g	N/A
Ethoprophos	Any amount	ND	0.00632 µg/g	0.01914 µg/g	Pass
Etofenprox	Any amount	ND	0.00604 µg/g	0.01831 µg/g	Pass
Etoxazole	0.1 µg/g	0.1463 µg/g	0.00363 µg/g	0.01099 µg/g	Fail
Fenhexamid	0.1 µg/g	ND	0.01344 µg/g	0.04073 µg/g	Pass
Fenoxycarb	Any amount	ND	0.0047 µg/g	0.01423 µg/g	Pass
Fenpyroximate	0.1 µg/g	0.4514 µg/g	0.00277 µg/g	0.0084 µg/g	Fail
Fipronil	Any amount	ND	0.00678 µg/g	0.02054 µg/g	Pass
Flonicamid	0.1 µg/g	ND	0.0046 µg/g	0.01393 µg/g	Pass
Fludioxonil	0.1 µg/g	ND	0.03245 µg/g	0.09834 µg/g	Pass
Hexythiazox	0.1 µg/g	0.1923 µg/g	0.00409 µg/g	0.01238 µg/g	Fail
Imazalil	Any amount	ND	0.012 µg/g	0.03637 µg/g	Pass
Imidacloprid	5 µg/g	0.0455 µg/g	0.00796 µg/g	0.02411 µg/g	Pass
Kresoxim- methyl	0.1 µg/g	ND	0.00989 µg/g	0.02997 µg/g	Pass
Malathion	0.5 µg/g	10.3562 µg/g	0.00701 µg/g	0.02124 µg/g	Fail

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Metalaxyl	2 µg/g	0.481 µg/g	0.0058 µg/g	0.01757 µg/g	Pass
Methiocarb	Any amount	ND	0.00885 µg/g	0.02681 µg/g	Pass
Methomyl	1 µg/g	ND	0.00837 µg/g	0.02537 µg/g	Pass
Mevinphos	Any amount	ND			Pass
Mevinphos I		ND	0.001 µg/g	0.00303 µg/g	N/A
Mevinphos II		ND	0.00529 µg/g	0.01603 µg/g	N/A
Myclobutanil	0.1 µg/g	6.5213 µg/g	0.01719 µg/g	0.0521 µg/g	Fail
Naled	0.1 µg/g	ND	0.01059 µg/g	0.0321 µg/g	Pass
Oxamyl	0.5 µg/g	ND	0.00617 µg/g	0.01869 µg/g	Pass
Paclobutrazol	Any amount	0.1184 µg/g	0.01076 µg/g	0.03262 µg/g	Fail
Permethrin	0.5 µg/g	1.7292 µg/g			Fail
Permethrin cis		1.0372 µg/g	0.00993 µg/g	0.03008 µg/g	N/A
Permethrin trans		0.692 µg/g	0.01265 µg/g	0.03833 µg/g	N/A
Phosmet	0.1 µg/g	ND	0.00601 µg/g	0.01822 µg/g	Pass
Piperonylbuto- xide	3 µg/g	2.113 µg/g	0.00261 µg/g	0.00791 µg/g	Pass
Prallethrin	0.1 µg/g	ND	0.00989 µg/g	0.02996 µg/g	Pass
Propiconazole	0.1 µg/g	0.0404 µg/g	0.00577 µg/g	0.01747 µg/g	Pass
Propoxur	Any amount	ND	0.00593 µg/g	0.01798 µg/g	Pass
Pyrethrins	0.5 µg/g	0.503 µg/g			Fail
Pyrethrins Pyrethrin I		0.4419 µg/g	0.00435 µg/g	0.01318 µg/g	N/A
Pyrethrins Pyrethrin II		0.0611 µg/g	0.00386 µg/g	0.01169 µg/g	N/A
Pyridaben	0.1 µg/g	0.1268 µg/g	0.00388 µg/g	0.01176 µg/g	Fail
Spinetoram	0.1 µg/g	ND			Pass
Spinetoram J		ND	0.00694 µg/g	0.02103 µg/g	N/A
Spinetoram L		ND	0.00902 µg/g	0.02734 µg/g	N/A
Spinosad	0.1 µg/g	ND			Pass
Spinosad A		ND	0.00799 µg/g	0.02422 µg/g	N/A
Spinosad D		ND	0.00275 µg/g	0.00834 µg/g	N/A
Spiromesifen	0.1 µg/g	0.2637 µg/g	0.00693 µg/g	0.021 µg/g	Fail
Spirotetramat	0.1 µg/g	ND	0.00537 µg/g	0.01627 µg/g	Pass
Spiroxamine	Any amount	ND	0.00549 µg/g	0.01663 µg/g	Pass
Tebuconazole	0.1 µg/g	0.264 µg/g	0.00874 µg/g	0.02647 µg/g	Fail
Thiacloprid	Any amount	ND	0.00458 µg/g	0.01389 µg/g	Pass
Thiamethoxam	5 µg/g	ND	0.00395 µg/g	0.01196 µg/g	Pass
Trifloxystrob- in	0.1 µg/g	0.3134 µg/g	0.00354 µg/g	0.01072 µg/g	Fail

BCL-020: Heavy Metal Testing by ICP-MS Jul 05, 2023

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
Arsenic	0.2 µg/g	< LOQ	0.001 µg/g	0.05 µg/g	Pass
Cadmium	0.2 µg/g	ND	0.0002 µg/g	0.05 µg/g	Pass
Lead	0.5 µg/g	< LOQ	0.0003 µg/g	0.05 µg/g	Pass
Mercury	0.1 µg/g	< LOQ	0.0001 µg/g	0.01 µg/g	Pass

BCL-07: Foreign Material Testing by Microscopy Jul 05, 2023

Analyte	Limit	Detected	Pass/Fail
Imbedded Foreign Material	25 %	ND	Pass
Insect Fragments, Hair, Mammal Excrement	1 Unit	ND	Pass
Mold	25 %	ND	Pass
Sand, Soil, Cinders, Dirt	25 %	ND	Pass

BCL-18: Residual Solvents Analysis by HS-GC-MS Jul 07, 2023

Analyte	Limit	Detected	LOD	LOQ	Pass/Fail
1,2- Dichloroethane	1 µg/g	ND	0.17152 µg/g	0.59832 µg/g	Pass
Acetone	5000 µg/g	ND	19.30594 µg/g	59.83247 µg/g	Pass
Acetonitrile	410 µg/g	ND	17.13203 µg/g	59.83247 µg/g	Pass
Benzene	1 µg/g	ND	0.07579 µg/g	0.59832 µg/g	Pass
Butane	5000 µg/g	189.102 µg/g	18.06542 µg/g	59.83247 µg/g	Pass
Chloroform	1 µg/g	ND	0.17551 µg/g	0.59832 µg/g	Pass
Ethanol	5000 µg/g	427.504 µg/g	14.81053 µg/g	59.83247 µg/g	Pass
Ethyl acetate	5000 µg/g	ND	18.28879 µg/g	59.83247 µg/g	Pass
Ethylene oxide	1 µg/g	ND	0.19146 µg/g	0.59832 µg/g	Pass
Ethyl ether	5000 µg/g	ND	16.11089 µg/g	59.83247 µg/g	Pass
Heptane	5000 µg/g	ND	14.09653 µg/g	59.83247 µg/g	Pass
Hexane	290 µg/g	ND	21.70323 µg/g	99.72078 µg/g	Pass
Isopropyl alcohol	5000 µg/g	ND	14.95812 µg/g	59.83247 µg/g	Pass
Methanol	3000 µg/g	ND	13.41444 µg/g	59.83247 µg/g	Pass
Methylene chloride	1 µg/g	ND	0.15158 µg/g	0.59832 µg/g	Pass
Pentane	5000 µg/g	ND	32.98763 µg/g	99.72078 µg/g	Pass
Propane	5000 µg/g	ND	17.04428 µg/g	59.83247 µg/g	Pass
Toluene	890 µg/g	ND	9.41763 µg/g	59.83247 µg/g	Pass
Trichloroethy- lene	1 µg/g	ND	0.07978 µg/g	0.59832 µg/g	Pass
o-Xylene		ND	4.45951 µg/g	29.91623 µg/g	N/A
p- and m-Xylene		ND	4.13243 µg/g	29.91623 µg/g	N/A
Total xylenes	2170 µg/g	ND			Pass

* For quality assurance purposes. Not a California compliance certificate.